Environmental Analytical Chemistry

Environmental Analytical Chemistry

Instructor:

Focus:

This road map was developed for an upper level chemistry course that serves as one of the advanced lab options.  The course is mostly an instrumental analysis course with a focus on environmental samples.  The majority of the course is laboratory based learning.  I have selected a group of papers that all relate to the instruments we use in the course.   The papers do not come from a single lab but rather focus on understanding the instruments, statistical analysis, and environmental implications.

Overview:

Applicable for Courses:

Educational Level:

Roadmap Objectives:

    • Article: Kratochvil, B.; Taylor, J. K. Sampling for Chemical Analysis. Analytical Chemistry 1981, 53, 924 A-938 A.
    • Content area/major concepts: I chose this paper as the starting paper for the module because it details how to collect samples which will be the first assignment in lab for the students. Also, it starts discussion on error analysis which will be important all semester.
      Environmental sample preparation, data analysis, statistical analysis.
    • Methods or technology used to obtain data: Sample preparation, error in sample collection, error analysis.
    • How the CREATE strategy was used:
    • Biggest teaching challenge: Completely new information to students, statistical analysis.
    • Article: Winefordner, J. D.; Long, G. L. Limit of Detection A Closer Look at the IUPAC Definition. Analytical Chemistry 1983, 55, 712 A-724 A.
    • Content area/major concepts: I chose this paper as the next in the module because it goes into greater detail than the previous paper about statistical analysis. It focuses on the limit of detection which is a technique the students will be required to learn for lecture and lab.

      Concepts: Limit of detection, data analysis, statistical analysis.
    • Methods or technology used to obtain data: Error analysis
    • How the CREATE strategy was used:
    • Biggest teaching challenge: Data analysis and statistical analysis.
    • Article: Sutton, P. M.; Athanasoulis, M.; Flessel, P.; Guirguis, G.; Haan, M.; Schlag, R.; Goldman, L. R. Lead Levels in the Household Environment of Children in Three High-Risk Communities in California. Environmental Research 1995, 68, 45-57.
    • Content area/major concepts: I chose this paper as the next in the module because it puts the sample collection and statistical analysis into practice. Also, it uses a flame AAS which is instrument that the students will use in lab. It also uses a similar method of sample preparation with paint samples for lead analysis to the one used in lab.

      Concepts/Content Reviewed: Environmental sample preparation, data analysis, lead contamination, and statistical analysis.
    • Methods or technology used to obtain data: Sample collection, error analysis, and flame atomic absorption spectroscopy.
    • How the CREATE strategy was used:
    • Biggest teaching challenge: Complicated data sets in tables, difficult statistically analysis.
    • Article: Miller-Ihli, N. J. Trace Element Determinations in Foods and Biological Samples Using Inductively Coupled Plasma Atomic Emission Spectrometry and Flame Atomic Absorption Spectrometry. Journal of Agriculture and Food Chemistry 1996, 44, 2675-2679.
    • Content area/major concepts: I chose this paper as the next in the module because it also uses Flame AAS and introduces GFAAS and ICP-AES which are three of the four instruments used in lab. It also has data from some of the elements students will examine in lab.

      Concepts/Content Reviewed: Environmental sample preparation, elemental food composition data, data analysis, and statistical analysis.
    • Methods or technology used to obtain data: Sample collection/preparation, error analysis, and flame atomic absorption spectroscopy, introduction to graphite furnace atomic absorption spectroscopy, inductively coupled plasma atomic emission spectroscopy.
    • How the CREATE strategy was used:
    • Biggest teaching challenge: Complicated data sets in tables, difficult statistically analysis.
    • Article: El-Ghawi, U. M. The Level of Trace Elements in Tripoli City Groundwater. Instrumentation Science and Technology 2005, 33, 609-617.
    • Content area/major concepts: I chose this paper as the next in the module because it uses AAS and ICP as well as IC, the last instrument used in lab . It also has data from most of the elements and inorganic ions that students will examine in lab.

      Concepts/Content Reviewed: Environmental sample preparation, groundwater data, data analysis, and statistical analysis.
    • Methods or technology used to obtain data: Sample collection/preparation, error analysis, AAS, ICP, and IC.
    • How the CREATE strategy was used:
    • Biggest teaching challenge: : Not enough information given for complete understanding
    • Article: Article
    • Content area/major concepts:
    • Methods or technology used to obtain data:
    • How the CREATE strategy was used:
    • Biggest teaching challenge:
    • Article: Grady, D. Unexpected Dangers Found in Low Levels of Lead. New York Times 1996, C9.
    • Content area/major concepts: I chose this news article because it talks about dangers of low levels of lead which is of great interest for an environmental prospective. It is also to show how news articles do not have all the information and the main source must be located.

    • Methods or technology used to obtain data: OSHA standards, sample collection.
    • How the CREATE strategy was used:
    • Biggest teaching challenge: Not enough information given for complete understanding
    • Article: Cheng, Y.; Schwartz, J.; Sparrow, D.; Aro, A.; Weiss, S. T.; Hu, H. Bone Lead and Blood Lead Levels in Relation to Baseline Blood Pressure and Prospective Development of Hypertension. American Journal of Epidemiology 2001, 153, 164-171.
    • Content area/major concepts: I chose this paper as the next in the module because it uses a new instrument and one we have previously covered. Also it highlights the dangers of even low level exposure. It also shows the dramatic difference between what a news article might claim and what is actually studied in research.

      Concepts/Content Reviewed: Hypertension, lead contamination, blood and bone sample preparation.
    • Methods or technology used to obtain data: K-shell x-ray fluorescence and atomic absorption spectroscopy.
    • How the CREATE strategy was used:
    • Biggest teaching challenge: Complicated data sets in tables, difficult statistically analysis.
    • Article: Wolstenholme, J.; Hessler, W. Low level, long exposure to lead linked to depression, anxiety in women. Environmental Health News,
    • Content area/major concepts: I chose this news article because it talks about dangers of low levels of lead just like the previous news article which is of great interest for an environmental prospective.
    • Methods or technology used to obtain data: Sample collection, X-ray fluorescence.
    • How the CREATE strategy was used:
    • Biggest teaching challenge:
    • Article: Eum, K-D.; Korrick, S. A.; Weuve, J.; Okereke, O.; Kubzansky, L. D.; Hu, H.; Weisskopf, M. G. Relation of Cumulative Low-Level Lead Exposure to Depressive and Phobic Anxiety Symptom Scores in Middle-Age and Elderly Women. Environmental Health Perspectives 2012, 120, 817-823.
    • Content area/major concepts: I chose this paper as the next in the module because it also highlights the dangers of low level lead exposure. It goes into more statistical analysis than the previous paper. Also, it shows the difference between what is reported in popular news articles versus actual research.

      Concepts/Content Reviewed: Depression and anxiety, lead contamination, bone sample preparation.
    • Methods or technology used to obtain data: K-shell x-ray fluorescence, statistical analysis.
    • How the CREATE strategy was used:
    • Biggest teaching challenge:

Advice for Using Module/Activity:

The first five papers were developed for the lecture component. The last three articles were used in the lab component.
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